116
edits
1RQW: Difference between revisions
m
no edit summary
mNo edit summary |
mNo edit summary |
||
| Line 5: | Line 5: | ||
Prior to flash cooling in liquid nitrogen at 100 K the crystals were soaked for a few seconds in a solution containing 1 M sodium bromide and 25% (v/v) glycerol. | Prior to flash cooling in liquid nitrogen at 100 K the crystals were soaked for a few seconds in a solution containing 1 M sodium bromide and 25% (v/v) glycerol. | ||
The peak and inflection datasets (360 images each) are available from the [http://www.embl-hamburg.de/Xray_Tutorial/ EMBL Hamburg] website (alternatively from [http://www.mx.bessy.de/bessy-ws/experiment2.html]). The XDS data reductions and (some of the) phasing calculations are [ | The peak and inflection datasets (360 images each) are available from the [http://www.embl-hamburg.de/Xray_Tutorial/ EMBL Hamburg] website (alternatively from [http://www.mx.bessy.de/bessy-ws/experiment2.html]). The XDS data reductions and (some of the) phasing calculations are [https://{{SERVERNAME}}/pub/xds-datared/1rqw here]. | ||
Data reduction was performed starting with the [[XDS.INP#MarCDD_225mm_.40_SLS.2C_BL_X06SA|template for the MarCCD 225]] detector, changing | Data reduction was performed starting with the [[XDS.INP#MarCDD_225mm_.40_SLS.2C_BL_X06SA|template for the MarCCD 225]] detector, changing | ||