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The verdict is clear: high mosaicity (> 0.5°) bad ISa, anomalous correlation > 30% only to about 5 A. The reason becomes clear if we load FRAME.cbf into [[XDS-Viewer]], and zoom in: | The verdict is clear: high mosaicity (> 0.5°) bad ISa, anomalous correlation > 30% only to about 5 A. The reason becomes clear if we load FRAME.cbf into [[XDS-Viewer]], and zoom in: | ||
[[File:3csl-frame.png]] | [[File:3csl-frame.png]] | ||
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RESOLUTION NUMBER OF REFLECTIONS COMPLETENESS R-FACTOR R-FACTOR COMPARED I/SIGMA R-meas Rmrgd-F Anomal SigAno Nano | RESOLUTION NUMBER OF REFLECTIONS COMPLETENESS R-FACTOR R-FACTOR COMPARED I/SIGMA R-meas Rmrgd-F Anomal SigAno Nano | ||
LIMIT OBSERVED UNIQUE POSSIBLE OF DATA observed expected Corr | LIMIT OBSERVED UNIQUE POSSIBLE OF DATA observed expected Corr | ||
8.28 26530 7039 7111 99.0% 4.4% 4.6% 26516 23.79 5.2% 3.7% 57% 1.526 3211 | 8.28 26530 7039 7111 99.0% 4.4% 4.6% 26516 23.79 5.2% 3.7% 57% 1.526 3211 | ||
5.90 48700 12589 12598 99.9% 8.7% 8.5% 48700 14.00 10.2% 9.2% 23% 1.052 5989 | 5.90 48700 12589 12598 99.9% 8.7% 8.5% 48700 14.00 10.2% 9.2% 23% 1.052 5989 |